- PII
- S30345588S0002337X25030067-1
- DOI
- 10.7868/S3034558825030067
- Publication type
- Article
- Status
- Published
- Authors
- Volume/ Edition
- Volume 61 / Issue number 5
- Pages
- 312-316
- Abstract
- In this work, a new approach to the synthesis of iron pentacarbonyl Fe(CO)₅ is studied, offering a more stable and less energy-intensive alternative to traditional methods for obtaining metal carbonyls—the inductive flow levitation (IFL). The IFL technology allows the process to be conducted at relatively low pressure (~5 bar). To optimize the synthesis of metal carbonyls, the reaction setup was modernized using a cryotrapping system, which consists of a quartz ampoule immersed in a Dewar vessel, maintained at a temperature of -40°C using a thermostat. During experiments, the composition of the resulting gas mixture was analyzed using gas chromatography and mass spectrometry methods, enabling high-precision identification and monitoring of the synthesized product directly during the reaction process.
- Keywords
- Date of publication
- 17.03.2025
- Year of publication
- 2025
- Number of purchasers
- 0
- Views
- 42
References
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